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Mixture of nitrobenzene and aniline can ...

Mixture of nitrobenzene and aniline can be separated by

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The mixture is treated with dil HCl. Only aniline dissolves.It is then shaken with ether. Nitrobenzene goes into ether layer. It is separated. Nitrobenzenne is obtained by evaporating ether. The aqueous layer, on neutralisation with NaOH gives aniline. It is also shaken with ether separately and ether is collected. Aniline is obtained by evaporating ether.
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